(Z)-3-[2-(2,4-Dinitrophenyl)hydrazin-1-ylidene]isobenzofuran-1(3H)-one dichloromethane hemisolvate

Palak Agarwal; Pragati Mishra; Nikita Gupta; Neelam; Priyaranjan Sahoo; Satish Kumar

doi:10.1107/S1600536814004929

Acta Crystallographica Section E (Apr 2014)

(Z)-3-[2-(2,4-Dinitrophenyl)hydrazin-1-ylidene]isobenzofuran-1(3H)-one dichloromethane hemisolvate

Palak Agarwal,
Pragati Mishra,
Nikita Gupta,
Neelam,
Priyaranjan Sahoo,
Satish Kumar

Affiliations

Palak Agarwal: Department of Chemistry, St. Stephen's College, University Enclave, Delhi, 110007, India
Pragati Mishra: Department of Chemistry, St. Stephen's College, University Enclave, Delhi, 110007, India
Nikita Gupta: Department of Chemistry, St. Stephen's College, University Enclave, Delhi, 110007, India
Neelam: Department of Chemistry, St. Stephen's College, University Enclave, Delhi, 110007, India
Priyaranjan Sahoo: Department of Chemistry, St. Stephen's College, University Enclave, Delhi, 110007, India
Satish Kumar: Department of Chemistry, St. Stephen's College, University Enclave, Delhi, 110007, India

DOI: https://doi.org/10.1107/S1600536814004929
Journal volume & issue: Vol. 70, no. 4
pp. o418 – o418

Abstract

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In the title compound, 2C14H8N4O6·CH2Cl2, the dichloromethane solvent molecule resides on a crystallographic twofold axis. The mean plane of the phthalisoimide ring is oriented at a dihedral angle of 32.93 (12)° with respect to the nitro-substituted benzene ring. An intramolecular N—H...O hydrogen bond occurs. The crystal packing features a short Cl...O halogen-bond interaction [3.093 (3) Å].

Published in Acta Crystallographica Section E

ISSN: 1600-5368 (Online)
Publisher: International Union of Crystallography
Country of publisher: United Kingdom
LCC subjects: Science: Chemistry: Crystallography
Website: https://journals.iucr.org/e/

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