Synthesis of novel 4-arylidene-benzodiazepines using Cellulose@SiPr@Catechin@Fe3O4

Tamila Shafaati; Mohammad Nikpassand; Masoud Mokhtary; Leila Zare Fekri

Results in Chemistry (Jan 2024)

Synthesis of novel 4-arylidene-benzodiazepines using Cellulose@SiPr@Catechin@Fe3O4

Tamila Shafaati,
Mohammad Nikpassand,
Masoud Mokhtary,
Leila Zare Fekri

Affiliations

Tamila Shafaati: Department of Chemistry, Rasht Branch, Islamic Azad University, Rasht, Iran
Mohammad Nikpassand: Department of Chemistry, Rasht Branch, Islamic Azad University, Rasht, Iran; Corresponding author.
Masoud Mokhtary: Department of Chemistry, Rasht Branch, Islamic Azad University, Rasht, Iran
Leila Zare Fekri: Department of Chemistry, Payame Noor University, PO Box 19395-3697 Tehran, Iran

Journal volume & issue: Vol. 7
p. 101525

Abstract

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This research work describes the synthesis and characterization of Cellulose@SiPr@Catechin@Fe3O4 nanocomposite, a novel and effective nanocatalyst in the synthesis of 1,5-benzodiazepine derivatives by reaction of 1,2-phenylenediamine, Meldrum's acid and azo aldehydes. 1H NMR, 13C NMR, and FTIR spectral data and mass analyses characterized all products. The nanocatalyst was characterized by fourier transform infrared spectroscopy (FT-IR), field emission scanning electron microscope (FE-SEM), transmission electron microscope (TEM), Brunauer–Emmett–Teller (BET), X-ray powder diffraction (XRD), X-ray spectroscopy (EDX), vibrating sample magnetometry (VSM), and thermogravimetric analysis (TGA).

Published in Results in Chemistry

ISSN: 2211-7156 (Online)
Publisher: Elsevier
Country of publisher: Netherlands
LCC subjects: Science: Chemistry
Website: https://www.journals.elsevier.com/results-in-chemistry/

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