Nanotechnology and Precision Engineering (Sep 2018)

Anisotropic brittle-ductile transition of monocrystalline sapphire during orthogonal cutting and nanoindentation experiments

  • Philipp Maas,
  • Yuta Mizumoto,
  • Yasuhiro Kakinuma,
  • Sangkee Min

Journal volume & issue
Vol. 1, no. 3
pp. 157 – 171

Abstract

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Single-crystal sapphire is utilized as a high-performance engineering material, especially in extreme and harsh environments. However, due to its extreme hardness and brittleness, the machinability of sapphire is still a challenge. By means of nanoindentation and plunge-cut experiments, the anisotropic brittle-ductile transition of the prismatic M-plane and rhombohedral R-plane is examined by analyzing crack morphologies and the critical depth-of-cut (CDC). The experimental results of the nanoindentation tests are correlated to the plunge-cut experiment. Both the prism plane and the rhombohedral crystal plane exhibit a two-fold symmetry of ductility with various crack patterns along the machined grooves. The direction-dependent plasticity of the hexagonal sapphire crystal is mainly connected to a twinning process accompanied by slip dislocation. Keywords: Sapphire, Anisotropy, Brittle-ductile transition, Orthogonal cutting