Synthesis and crystal structure of 7-chloro-2-(ethylsulfinyl)-6-fluoro-3-(1H-pyrazole-1-yl)-4H-thiochromen-4-one, C13H10FN3OS2

Zhang Yuming; Xiao Tao; Guo Xuan; Dou Chaolong; Wu Wenyuan

doi:10.1515/ncrs-2019-0243

Zeitschrift für Kristallographie - New Crystal Structures (Sep 2019)

Synthesis and crystal structure of 7-chloro-2-(ethylsulfinyl)-6-fluoro-3-(1H-pyrazole-1-yl)-4H-thiochromen-4-one, C13H10FN3OS2

Zhang Yuming,
Xiao Tao,
Guo Xuan,
Dou Chaolong,
Wu Wenyuan

Affiliations

Zhang Yuming: Department of Chemistry and Molecular Engineering, Nanjing Tech University, 30 Puzhu South Road, Nanjing 211816, China
Xiao Tao: Department of Chemistry and Molecular Engineering, Nanjing Tech University, 30 Puzhu South Road, Nanjing 211816, China
Guo Xuan: Department of Chemistry and Molecular Engineering, Nanjing Tech University, 30 Puzhu South Road, Nanjing 211816, China
Dou Chaolong: Department of Chemistry and Molecular Engineering, Nanjing Tech University, 30 Puzhu South Road, Nanjing 211816, China
Wu Wenyuan: Department of Chemistry and Molecular Engineering, Nanjing Tech University, 30 Puzhu South Road, Nanjing 211816, China

DOI: https://doi.org/10.1515/ncrs-2019-0243
Journal volume & issue: Vol. 234, no. 5
pp. 1033 – 1034

Abstract

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C14H10ClFN2O2S2, monoclinic, P21/n (no. 14), a = 15.070(3) Å, b = 4.9050(10) Å, c = 21.018(4) Å, β = 105.59(3)°, V = 1496.5(5) Å3, Z = 4, Rgt(F) = 0.0667, wRref(F2) = 0.1363, T = 293(2) K.

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Published in Zeitschrift für Kristallographie - New Crystal Structures

ISSN: 1433-7266 (Print); 2197-4578 (Online)
Publisher: De Gruyter
Country of publisher: Germany
LCC subjects: Science: Physics; Science: Chemistry: Crystallography
Website: https://www.degruyter.com/journal/key/ncrs/html

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