Preparation and characterization of rice husk activated carbon-supported zinc oxide nanocomposite (RHAC-ZnO-NC)

Abstract

Indiscriminate waste discharge into water bodies has increased the level of water pollution via anthropogenic activities. Hence the need for the development of sustainable and environmentally benign nanomaterials has the potential for wastewater treatment. Rice husk activated carbon (RHAC) prepared by orthophosphoric acid activation was successfully loaded with freshly prepared ZnO nanoparticles by a bottom-up approach via precipitation method resulting in the RHAC-ZnO-NC. RHAC-ZnO-NC's mineralogy with 72% zincite was determined by XRD, morphology by SEM, and the functional group by FTIR. The physicochemical parameters showed surface area 615.2 m2 g-1, pH (pzc) (6.62), pH (6.53), bulk density (0.88 g/cm3), ash content (18.45%), and volatile matter (58.08%). The porosity was determined by iodine number. Boehm titration was carried out for oxygen-bearing functional group determination. The study substantiated RHAC-ZnO-NC as a promising material for adsorption and photocatalytic degradation.

Keywords

• Zinc oxide
• Nanocomposites
• Rice husk
• Activated carbon
• Characterization