2,3,5-<i>Tri</i>-<i>O</i>-benzyl-<span style="font-variant: small-caps">d</span>-xylofuranose

Abstract

The synthesis and crystallization of 2,3,5-tri-O-benzyl-d-xylofuranose permitted us to isolate the alpha anomer with a small contamination of the beta form (ca 10%), whose first crystallographic structure obtained in the P212121 space group was determined at 100 K up to a resolution of sin θmax/λ = 0.71 Å−1 and refined to an R1 value of 0.0171 with a Hirshfeld atom refinement (HAR) approach.

Keywords

• d-xylofuranose%22%2C%22default_operator%22%3A%22AND%22%7D%7D%7D"> 2,3,5-<i>tri</i>-<i>O</i>-benzyl-<span style="font-variant: small-caps">d</span>-xylofuranose
• synthesis
• Hirshfeld atom refinement of X-ray structure
• 3-D Hirshfeld surface
• crystal packing