Gravimetric Separation of Heavy Minerals in Sediments and Rocks

Abstract

The potential of heavy minerals studies in provenance analysis can be enhanced conspicuously by using a state-of-the-art protocol for sample preparation in the laboratory, which represents the first fundamental step of any geological research. The classical method of gravimetric separation is based on the properties of detrital minerals, principally their grain size and density, and its efficiency depends on the procedure followed and on the technical skills of the operator. Heavy-mineral studies in the past have been traditionally focused on the sand fraction, generally choosing a narrow grain-size window for analysis, an approach that is bound to introduce a serious bias by neglecting a large, and sometimes very large, part of the heavy-mineral spectrum present in the sample. In order to minimize bias, not only the largest possible size range in each sample should be considered, but also, the same quantitative analytical methods should be applied to the largest possible grain-size range occurring in the sediment system down to 5 μm or less, thus including suspended load in rivers, loess deposits, and shallow to deep-marine muds. Wherever the bulk sample cannot be used for practical reasons, we need to routinely analyze the medium silt to medium sand range (15−500 μm) for sand and the fine silt to sand range (5−63 or > 63 μm) for silt. This article is conceived as a practical handbook dedicated specifically to Master and PhD students at the beginning of their heavy-mineral apprenticeship, as to more expert operators from the industry and academy to help improving the quality of heavy-mineral separation for any possible field of application.

Keywords

• handbook for laboratory procedures
• nontoxic heavy liquids
• wet sieving of silt
• size-window for analysis
• zircon separation
• heavy-mineral mounts
• provenance analysis