N-(4-Chlorophenyl)-4-methoxy-3-(propanamido)benzamide cyclohexane hemisolvate

Abstract

The title compound, C17H17ClN2O3·0.5C6H12, was prepared by the condensation reaction of 4-methoxy-3-(propanamido)benzoic acid with 4-chloroaniline. The Cl atom, the propionyl CH3 group and the cyclohexyl CH2 group are disordered over two sets of sites of equal occupancy in both molecules. The cyclohexane solvent molecule is disordered over two orientations which were modelled with relative occupancies of 0.484 (4) and 0.516 (4). In the crystal, there are a number of N—H...O hydrogen bonds, forming layers perpendicular to (001).