Beilstein Journal of Organic Chemistry (Feb 2019)

Low-budget 3D-printed equipment for continuous flow reactions

  • Jochen M. Neumaier,
  • Amiera Madani,
  • Thomas Klein,
  • Thomas Ziegler

DOI
https://doi.org/10.3762/bjoc.15.50
Journal volume & issue
Vol. 15, no. 1
pp. 558 – 566

Abstract

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This article describes the development and manufacturing of lab equipment, which is needed for the use in flow chemistry. We developed a rack of four syringe pumps controlled by one Arduino computer, which can be manufactured with a commonly available 3D printer and readily available parts. Also, we printed various flow reactor cells, which are fully customizable for each individual reaction. With this equipment we performed some multistep glycosylation reactions, where multiple 3D-printed flow reactors were used in series.

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