Nanomaterials (Jan 2024)

Laboratory X-ray Microscopy of 3D Nanostructures in the Hard X-ray Regime Enabled by a Combination of Multilayer X-ray Optics

  • Bartlomiej Lechowski,
  • Kristina Kutukova,
  • Joerg Grenzer,
  • Iuliana Panchenko,
  • Peter Krueger,
  • Andre Clausner,
  • Ehrenfried Zschech

DOI
https://doi.org/10.3390/nano14020233
Journal volume & issue
Vol. 14, no. 2
p. 233

Abstract

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High-resolution imaging of buried metal interconnect structures in advanced microelectronic products with full-field X-ray microscopy is demonstrated in the hard X-ray regime, i.e., at photon energies > 10 keV. The combination of two multilayer optics—a side-by-side Montel (or nested Kirkpatrick–Baez) condenser optic and a high aspect-ratio multilayer Laue lens—results in an asymmetric optical path in the transmission X-ray microscope. This optics arrangement allows the imaging of 3D nanostructures in opaque objects at a photon energy of 24.2 keV (In-Kα X-ray line). Using a Siemens star test pattern with a minimal feature size of 150 nm, it was proven that features 6Sn5/Cu microbump interconnects fabricated using solid–liquid interdiffusion (SLID) bonding.

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