Construção de espectrômetro de emissão atômica com atomização eletrotérmica em filamento de tungstênio (WCAES) Construction of a tungsten coil atomic emission spectrometer (WCAES)

Abstract

It is here discussed the development of a low cost analytical instrument with capacity for metals determination using atomic emission measurements in an electrothermal atomization system with a tungsten coil atomizer. The main goal was to show a new frontier for using this atomizer and to demonstrate that the simple instrumental arrangement here proposed has potential for portability and for solving analytical tasks related to metals determination. Atomic emission of calcium was selected for the adjustment of instrumental parameters and to evaluate the main characteristics of the lab-built instrument. Cobalt was determined in medicines and one alloy to demonstrate its feasibility.

Keywords

• atomic emission spectrometry
• tungsten coil atomic emission spectrometry (WCAES)
• instrumentation