مجلة جامعة الانبار للعلوم الصرفة (Jun 2012)

Synthesis compounds of Thiopyran Pyridinium Perchlorate and studing its Bioactivity: Part1.

  • Marwan Mohammed Farhan

DOI
https://doi.org/10.37652/juaps.2009.15380
Journal volume & issue
Vol. 3, no. 2
pp. 76 – 87

Abstract

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A synthesis Four Pyridinium perchlorate Compounds from reaction one mole pyrylium salt (product already) with one mole 2-Aminoethylenethiol in room temp. and diagnosing them by Spectrally (FTI.R., 1H.N.M.R.) in addition to the accurate quantitative elemental analysis. A synthesis sixteen Thiopyranpyridiniumperchlorate Compounds from reaction one mole from Pyridinium compounds Produced with one mole pyrylium salt (product already) in under zero temp. very good yields and diagnosing them by pectrally (FTI.R., 1H.N.M.R.) in addition to the accurate quantitative elemental analysis. A should Molecular Weight for Synthesis compounds By using down Freeze Degree apparition Molecular Weight for Synthesis compounds compared to Molecular Weight cast. Studying the antimicrobial activity of the synthesized compound was tested against Gram positive and Gram negative bacteria and some fungi and have high good effect upon some becteria and fungi. This method provides several advantages such as very good yield, simple work-up procedure and environment friendly and compounds it more important in the field of medicinal and synthesis it.

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