Metals (Oct 2019)
Influence of Thermal and Magnetic History on Direct Δ<i>T<sub>ad</sub></i> Measurements of Ni<sub>49+x</sub>Mn<sub>36−x</sub>In<sub>15</sub> Heusler Alloys
Abstract
In the present work, using Heusler Ni49+xMn36-xIn15 (with x = 0 and 0.5) alloys, it is shown that the choice of the appropriate measurement protocol (erasing the prior state of the sample in between experiments) in ∆Tad first shot characterization is crucial for obtaining reliable results. Unlike indirect measurements, for which incorrect protocols produce overestimates of the characteristics of the material, erroneous direct measurements underestimate ∆Tad in the region close to its first order phase transition. The error in ∆Tad is found to be dependent on the temperature step used, being up to ~40% underestimation, including a slight shift in its peak temperature.
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