Detection of Methamphetamine using Nanobentonite as a Novel Solid Phase Extraction Column Matrix Assisted with Gas Chromatography- Mass Spectroscopy

Nur Asyiah Dalimunthe; Zul Alfian; Basuki Wirjosentono; Eddiyanto

doi:10.21123/bsj.2022.19.4.0816

Baghdad Science Journal (Aug 2022)

Detection of Methamphetamine using Nanobentonite as a Novel Solid Phase Extraction Column Matrix Assisted with Gas Chromatography- Mass Spectroscopy

Nur Asyiah Dalimunthe,
Zul Alfian,
Basuki Wirjosentono,
Eddiyanto

Affiliations

Nur Asyiah Dalimunthe: Postgraduate School, Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Sumatera Utara, Jl. Bioteknologi No. 1, Medan 20155, Indonesia & Department of Agritechnology, Faculty of Agriculture, Universitas Medan Area, Jalan Kolam No. 1, Medan, 20223, North Sumatera, Indonesia
Zul Alfian: Postgraduate School, Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Sumatera Utara, Jl. Bioteknologi No. 1, Medan 20155, Indonesia & Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Sumatera Utara, Jl. Bioteknologi No. 1, Medan 20155, Indonesia
Basuki Wirjosentono: Postgraduate School, Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Sumatera Utara, Jl. Bioteknologi No. 1, Medan 20155, Indonesia & Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Sumatera Utara, Jl. Bioteknologi No. 1, Medan 20155, Indonesia
Eddiyanto: Postgraduate School, Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Sumatera Utara, Jl. Bioteknologi No. 1, Medan 20155, Indonesia & Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Negeri Medan, Indonesia

DOI: https://doi.org/10.21123/bsj.2022.19.4.0816
Journal volume & issue: Vol. 19, no. 4

Abstract

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This study was done to evaluate a new technique to determine the presence of methamphetamine in the hair using nano bentonite-based adsorbent as the filler of extraction column. The state of the art of this study was based on the presence of silica in the nano bentonite that was assumed can interact with methamphetamine. The hair used was treated using methanol to extract the presence of methamphetamine, then it was continued by sonicating the hair sample. Qualitative analysis using Marquish reagent was performed to confirm the presence of methamphetamine in the isolate.The hair sample that has been taken in a different period confirmed that this current developing method can be used to analyzed methamphetamine. This method has an average recovery percentage by 104%. This result was also supported by the precision, linearity, LOD and LOQ, i.e. 0.0775; 0.968; 0.00000256 and 0.000000775, respectively.

Extraction column, Hair, Methamphetamine,Nanobentonite

Published in Baghdad Science Journal

ISSN: 2078-8665 (Print); 2411-7986 (Online)
Publisher: College of Science for Women, University of Baghdad
Country of publisher: Iraq
LCC subjects: Science
Website: http://bsj.uobaghdad.edu.iq/index.php/BSJ

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