Crystal structure of S-hexyl (E)-3-(4-methoxybenzylidene)dithiocarbazate

M. S. Begum; M. B. H. Howlader; R. Miyatake; E. Zangrando; M. C. Sheikh

doi:10.1107/S2056989015003199

Acta Crystallographica Section E: Crystallographic Communications (Mar 2015)

Crystal structure of S-hexyl (E)-3-(4-methoxybenzylidene)dithiocarbazate

M. S. Begum,
M. B. H. Howlader,
R. Miyatake,
E. Zangrando,
M. C. Sheikh

Affiliations

M. S. Begum: Department of Chemistry, Rajshahi University, Rajshahi-6205, Bangladesh
M. B. H. Howlader: Department of Chemistry, Rajshahi University, Rajshahi-6205, Bangladesh
R. Miyatake: Center for Environmental Conservation and Research Safety, University of Toyama, 3190 Gofuku, Toyama 930-8555, Japan
E. Zangrando: Department of Chemical and Pharmaceutical Sciences, Via Giorgieri 1, 34127 Trieste, Italy
M. C. Sheikh: Department of Applied Chemistry, Faculty of Engineering, University of Toyama, 3190 Gofuku, Toyama, 930-8555, Japan

DOI: https://doi.org/10.1107/S2056989015003199
Journal volume & issue: Vol. 71, no. 3
pp. o199 – o199

Abstract

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In the title compound, C15H22N2OS2, the dithiocarbazate group adopts an EE conformation with respect to the C=N bond of the benzylidene moiety. The hexyl side chain adopts an extended conformation and the C—S—C—C torsion angle is −93.36 (13)°. In the crystal, inversion dimers linked by pairs of N—H...S hydrogen bonds generate R22(8) loops.

Published in Acta Crystallographica Section E: Crystallographic Communications

ISSN: 2056-9890 (Online)
Publisher: International Union of Crystallography
Country of publisher: United Kingdom
LCC subjects: Science: Chemistry: Crystallography
Website: https://journals.iucr.org/e/

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