Crystal structures of the methylene chloride disolvates of tetrakis(3,5- dimethoxyphenyl)porphyrin and its isotypic copper(II) and nickel(II) complexes, C52H46N4O8 · 2CH2Cl2, Cu(C52H44N4O8) · 2CH2Cl2, Ni(C52H44N4O8) · 2CH2Cl2

Zeller M.; DiMuzio S. J.; Bee K.; Clemente J.; Frederick J.; Fucci A.; Gordon L.; Harper A.; Kasmar A.; Kasmar C.; Polomsky S.; Simmons A.; Smallsreed D.; Underwood T.; Hunter A. D.

doi:10.1524/ncrs.2006.221.1.15

Zeitschrift für Kristallographie - New Crystal Structures (Mar 2006)

Crystal structures of the methylene chloride disolvates of tetrakis(3,5- dimethoxyphenyl)porphyrin and its isotypic copper(II) and nickel(II) complexes, C52H46N4O8 · 2CH2Cl2, Cu(C52H44N4O8) · 2CH2Cl2, Ni(C52H44N4O8) · 2CH2Cl2

Zeller M.,
DiMuzio S. J.,
Bee K.,
Clemente J.,
Frederick J.,
Fucci A.,
Gordon L.,
Harper A.,
Kasmar A.,
Kasmar C.,
Polomsky S.,
Simmons A.,
Smallsreed D.,
Underwood T.,
Hunter A. D.

Affiliations

Zeller M.: Youngstown State University, STaRBURSTT-Cyberdiffraction Consortium @ YSU & Department of Chemistry, 1 University Plaza, Youngstown, OH 44555-3663, USA
DiMuzio S. J.: LaBrae High School, 1001 N. Leavitt Road, Leavittsburg, OH 44430, USA
Bee K.: LaBrae High School, 1001 N. Leavitt Road, Leavittsburg, OH 44430, USA
Clemente J.: LaBrae High School, 1001 N. Leavitt Road, Leavittsburg, OH 44430, USA
Frederick J.: LaBrae High School, 1001 N. Leavitt Road, Leavittsburg, OH 44430, USA
Fucci A.: Youngstown State University, STaRBURSTT-Cyberdiffraction Consortium @ YSU & Department of Chemistry, 1 University Plaza, Youngstown, OH 44555-3663, USA
Gordon L.: LaBrae High School, 1001 N. Leavitt Road, Leavittsburg, OH 44430, USA
Harper A.: LaBrae High School, 1001 N. Leavitt Road, Leavittsburg, OH 44430, USA
Kasmar A.: LaBrae High School, 1001 N. Leavitt Road, Leavittsburg, OH 44430, USA
Kasmar C.: LaBrae High School, 1001 N. Leavitt Road, Leavittsburg, OH 44430, USA
Polomsky S.: LaBrae High School, 1001 N. Leavitt Road, Leavittsburg, OH 44430, USA
Simmons A.: LaBrae High School, 1001 N. Leavitt Road, Leavittsburg, OH 44430, USA
Smallsreed D.: LaBrae High School, 1001 N. Leavitt Road, Leavittsburg, OH 44430, USA
Underwood T.: LaBrae High School, 1001 N. Leavitt Road, Leavittsburg, OH 44430, USA
Hunter A. D.: Youngstown State University, STaRBURSTT-Cyberdiffraction Consortium @ YSU & Department of Chemistry, 1 University Plaza, Youngstown, OH 44555-3663, USA

DOI: https://doi.org/10.1524/ncrs.2006.221.1.15
Journal volume & issue: Vol. 221, no. 1
pp. 15 – 19

Abstract

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C54H50Cl4N4O8, triclinic, P1̅ (no. 2), a = 11.295(1) Å, b = 11.255(1) Å, c = 11.797(1) Å, α = 108.904(2)°, β = 101.091(2)°, γ = 110.992(2)°, V = 1241.4 Å3, Z = 1, Rgt(F) = 0.056, wRref(F2) = 0.135, T = 100 K.

Published in Zeitschrift für Kristallographie - New Crystal Structures

ISSN: 1433-7266 (Print); 2197-4578 (Online)
Publisher: De Gruyter
Country of publisher: Germany
LCC subjects: Science: Physics; Science: Chemistry: Crystallography
Website: https://www.degruyter.com/journal/key/ncrs/html

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