Comparison between Biaxial Flexural Strength and Microstructure of Polished and Glaze-Fired Specimens of Zirconia Lithium Silicate Glass Ceramic

Abstract

Introduction: There has been a growing interest in glass ceramic systems with good esthetics, high fracture resistance, bonding durability, and simplified fabrication techniques using CAD/CAM. The aim of this study was to compare flexural strength in "polished" and "glazed and fired" specimens of zirconium lithium silicate (ZLS) CAD/CAM blocks Celtra Duo. Methods: A total of 14 specimens of Celtra Duo (Dentsply Sirona, Germany) were designated and equally divided into two groups, including group I (n=7; as polished) and group II (n=7; as glazed and fired) according to the manufacturers’ instructions. Then biaxial flexural strength was tested according to ISO 6872 using a universal testing machine and piston-on-three-ball method after polishing, glazing, and firing. The fractured surfaces and microstructure were observed by scanning electron microscope (Jeol/GSM5300). Data were then statistically analyzed using SPSS software (version 20.0). Results: There were statistically significant differences in biaxial flexural strength between a polished and glaze-fired specimen of ZLS glass ceramic discs as biaxial flexural strength was lower in polished specimens (mean±standard deviation: 158.7±21.67 MPa), while the glazed specimens showed higher biaxial flexural strength (mean±standard deviation: 261.5±31.89 MPa). Conclusion: Glazing and firing of Celtra Duo specimens increased biaxial flexural strength significantly in comparison to polishing with no significant change in the microstructure.

Keywords

• Celtra Duo
• Piston-on-three-ball
• CAD/CAM
• ZLS