Polymer Testing (Jan 2023)

Dynamic observation of a damping material using micro X-ray computed tomography coupled with a phase-locked loop

  • Masami Matsubara,
  • Taichi Komatsu,
  • Ryo Takara,
  • Masakazu Kobayashi,
  • Shogo Furuta,
  • Kentaro Uesugi,
  • Asahiro Nagatani,
  • Shozo Kawamura,
  • Daiki Tajiri

Journal volume & issue
Vol. 117
p. 107810

Abstract

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As rubber materials are used for damping, clarifying the relationship between the loss factor and microstructure would help develop high-performance damping materials. Although nondestructive observations using X-ray computed tomography (CT) under repetitive deformation have been reported, no observations have been reported at the submicron order that capture low-strain deformation, such as vibration exposure. The internal deformation behavior of materials with different loss factors has not yet been evaluated. This study proposes a dynamic X-ray CT method for specimens under tensile amplitudes, directly evaluating the internal deformation behavior of materials under dynamic conditions. The proposed 4D-CT has an excitation of 1 Hz and a spatial resolution of 0.5 μm. The local strain was obtained from X-ray CT at each phase, and the deformation behavior was evaluated. The results revealed that the peak of the local strain amplitude distribution curve decreased and the distribution widened as fine particles were mixed.

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