Molbank (Apr 2024)

5,5′-Thiobis(3-bromoisothiazole-4-carbonitrile)

  • Andreas S. Kalogirou,
  • Panayiotis A. Koutentis

DOI
https://doi.org/10.3390/M1813
Journal volume & issue
Vol. 2024, no. 2
p. M1813

Abstract

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The reaction of sodium 2,2-dicyanoethene-1,1-bis(thiolate) with bromine (2 equiv.) in CCl4 gave 3,5-dibromoisothiazole-3-carbonitrile and 5,5′-thiobis(3-bromoisothiazole-4-carbonitrile) in 7% and 18% yields, respectively. The latter novel compound was fully characterized.

Keywords