Separations (May 2024)

Early Identification of Olive Oil Defects throughout Shelf Life

  • Flávia Freitas,
  • Maria João Cabrita,
  • Marco Gomes da Silva

DOI
https://doi.org/10.3390/separations11060167
Journal volume & issue
Vol. 11, no. 6
p. 167

Abstract

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The unique aroma and flavor of extra virgin olive oil (EVOO) are generally associated with its volatile composition, which includes a variety of components responsible for positive attributes as well as sensory defects which result from chemical oxidation processes and the action of exogenous enzymes. In this study, a robust analytical method, headspace solid-phase microextraction combined with gas chromatography–mass spectrometry (HS-SPME-GC/MS), was developed to tentatively identify volatile organic compounds (VOCs) as markers of positive and negative attributes, correlating them with relative percentages to estimate the risk of disqualification during the shelf life of EVOO. Significant differences (p E-2-hexenal to acetic acid allowed for the prediction of the disqualification of monovarietal EVOO by the sensory panel.

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