Crystals (Jun 2021)

Laboratory-Based Nano-Computed Tomography and Examples of Its Application in the Field of Materials Research

  • Dominik Müller,
  • Jonas Graetz,
  • Andreas Balles,
  • Simon Stier,
  • Randolf Hanke,
  • Christian Fella

DOI
https://doi.org/10.3390/cryst11060677
Journal volume & issue
Vol. 11, no. 6
p. 677

Abstract

Read online

In a comprehensive study, we demonstrate the performance and typical application scenarios for laboratory-based nano-computed tomography in materials research on various samples. Specifically, we focus on a projection magnification system with a nano focus source. The imaging resolution is quantified with common 2D test structures and validated in 3D applications by means of the Fourier Shell Correlation. As representative application examples from nowadays material research, we show metallization processes in multilayer integrated circuits, aging in lithium battery electrodes, and volumetric of metallic sub-micrometer fillers of composites. Thus, the laboratory system provides the unique possibility to image non-destructively structures in the range of 170–190 nanometers, even for high-density materials.

Keywords