A Methodology Study on the Optimal Detection of Oil and Moisture Content in Soybeans Using LF-NMR and Its 2D <i>T</i>₁-<i>T</i>₂ Nuclear Magnetic Technology

Abstract

In this study, we aimed to provide an accurate method for the detection of oil and moisture content in soybeans. Introducing two-dimensional low-field nuclear magnetic resonance (LF-2D-NMR) qualitatively solved the problem of overlapping component signals that one-dimensional (1D) LF-NMR techniques cannot distinguish in soybean detection research. Soxhlet extraction, oven drying, LF-NMR spectrum, and LF-NMR oil and moisture content software were used to detect soybean oil and moisture content. The comparison showed that the LF-NMR oil and moisture content software was faster and more accurate than the other methods. The specific identification of the oil and moisture signals of soybean seeds using longitudinal relaxation time (T1) and transverse relaxation time (T2) successfully solved the problems of less mobile water, overlapping free water, and oil signals. Therefore, LF-2D-NMR can complement conventional LF-NMR assays, and this study provides a new method for the analysis and detection of moisture and oil in soybeans.

Keywords

• <i>T</i>₁-<i>T</i>₂
• LF-NMR
• LF-2D-NMR
• soybean
• oil and moisture content