Current Chemistry Letters (Jan 2024)

Sulfated tungstate: A highly efficient, recyclable and ecofriendly catalyst for synthesis of Flavones under the solvent-free conditions

  • Ajit P. Ingale,
  • Santosh T. Shinde,
  • Nitin M. Thorat

DOI
https://doi.org/10.5267/j.ccl.2024.1.006
Journal volume & issue
Vol. 13, no. 3
pp. 603 – 610

Abstract

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Sulfated tungstate efficiently catalyzes the cyclodehydration of 1-(2-hydroxyphenyl)-3-aryl-1,3-propanediones to flavones under solvent-free conditions. Utilization of conventional heating, simple reaction conditions, short reaction time, ease of product isolation and purification makes this manipulation very interesting from an economic and environmental perspective. Under these conditions, twelve examples were obtained with good yields (85-94%).